Information card for entry 4112130

Structure parameters

• Formula: C32 H88 Ho2 N6 O2 Si8
• Calculated formula: C32 H88 Ho2 N6 O2 Si8
• SMILES: C[Si](C)(C)N([Ho]1(N([Si](C)(C)C)[Si](C)(C)C)([O]2CCCC2)[N]2=[N]1[Ho]2(N([Si](C)(C)C)[Si](C)(C)C)(N([Si](C)(C)C)[Si](C)(C)C)[O]1CCCC1)[Si](C)(C)C
• Title of publication: Reduction of Dinitrogen to Planar Bimetallic M2(μ-η2:η2-N2) Complexes of Y, Ho, Tm, and Lu Using the K/Ln[N(SiMe3)2]3 Reduction System
• Authors of publication: William J. Evans; David S. Lee; Joseph W. Ziller
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2004
• Journal volume: 126
• Pages of publication: 454 - 455
• a: 10.8135 ± 0.0004 Å
• b: 23.4721 ± 0.0009 Å
• c: 11.546 ± 0.0004 Å
• α: 90°
• β: 112.587 ± 0.001°
• γ: 90°
• Cell volume: 2705.77 ± 0.17 ų
• Cell temperature: 172 ± 2 K
• Ambient diffraction temperature: 172 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0296
• Residual factor for significantly intense reflections: 0.0223
• Weighted residual factors for significantly intense reflections: 0.0473
• Weighted residual factors for all reflections included in the refinement: 0.0501
• Goodness-of-fit parameter for all reflections included in the refinement: 1.048
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No