Crystallography Open Database

Information card for entry 4112191

Preview

Coordinates	4112191.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C20.5 H46 B2 Br Cl P2
Calculated formula	C20.5 H46 B2 Br Cl P2
Title of publication	Radical-Type Reactivity of the 1,3-Dibora-2,4-Diphosphoniocyclobutane-1,3-diyl
Authors of publication	Hideki Amii; Lidija Vranicar; Heinz Gornitzka; Didier Bourissou; Guy Bertrand
Journal of publication	Journal of the American Chemical Society
Year of publication	2004
Journal volume	126
Pages of publication	1344 - 1345
a	19.684 ± 0.002 Å
b	10.1828 ± 0.0011 Å
c	14.0169 ± 0.0016 Å
α	90°
β	110.408 ± 0.002°
γ	90°
Cell volume	2633.2 ± 0.5 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	13
Hermann-Mauguin space group symbol	P 1 2/c 1
Hall space group symbol	-P 2yc
Residual factor for all reflections	0.0377
Residual factor for significantly intense reflections	0.0301
Weighted residual factors for significantly intense reflections	0.072
Weighted residual factors for all reflections included in the refinement	0.0761
Goodness-of-fit parameter for all reflections included in the refinement	1.033
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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