Information card for entry 4112241

Structure parameters

• Common name: [BVi4]-[MePPh3]+
• Formula: C27 H30 B P
• Calculated formula: C27 H30 B P
• Title of publication: The Tetra(vinyl)phosphonium Cation [(CH2CH)4P]+
• Authors of publication: Uwe V. Monkowius; Stefan D. Nogai; Hubert Schmidbaur
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2004
• Journal volume: 126
• Pages of publication: 1632 - 1633
• a: 10.3108 ± 0.0001 Å
• b: 14.585 ± 0.0002 Å
• c: 15.6994 ± 0.0003 Å
• α: 90°
• β: 100.11 ± 0.0006°
• γ: 90°
• Cell volume: 2324.26 ± 0.06 ų
• Cell temperature: 143 ± 2 K
• Ambient diffraction temperature: 143 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0449
• Residual factor for significantly intense reflections: 0.0419
• Weighted residual factors for significantly intense reflections: 0.1009
• Weighted residual factors for all reflections included in the refinement: 0.1031
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No