Crystallography Open Database

Information card for entry 4112379

Preview

Coordinates	4112379.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C40 H31 B F20 P2 W
Calculated formula	C41 H29 B F20 P2 W
Title of publication	Synthons for Coordinatively Unsaturated Complexes of Tungsten, and Their Use for the Synthesis of High Oxidation-State Silylene Complexes
Authors of publication	Benjamin V. Mork; T. Don Tilley
Journal of publication	Journal of the American Chemical Society
Year of publication	2004
Journal volume	126
Pages of publication	4375 - 4385
a	15.2193 ± 0.0002 Å
b	15.9706 ± 0.0002 Å
c	17.2664 ± 0.0003 Å
α	90°
β	96.322 ± 0.001°
γ	90°
Cell volume	4171.27 ± 0.11 Å³
Cell temperature	153.2 K
Ambient diffraction temperature	153.2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0668
Residual factor for significantly intense reflections	0.0415
Weighted residual factors for all reflections	0.05
Weighted residual factors for significantly intense reflections	0.0449
Goodness-of-fit parameter for all reflections included in the refinement	1.393
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4112379.html