Information card for entry 4112469

Structure parameters

• Formula: C82.5 H206 B22 P6 Rh6
• Calculated formula: C82.5 H206 B22 P6 Rh6
• Title of publication: [(iPr3P)6Rh6H12]2+: A High-Hydride Content Octahedron that Bridges the Gap between Late and Early Transition Metal Clusters
• Authors of publication: Michael J. Ingleson; Mary F. Mahon; Paul R. Raithby; Andrew S. Weller
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2004
• Journal volume: 126
• Pages of publication: 4784 - 4785
• a: 21.503 ± 0.0001 Å
• b: 25.489 ± 0.0001 Å
• c: 21.825 ± 0.0001 Å
• α: 90°
• β: 103.3°
• γ: 90°
• Cell volume: 11641.2 ± 0.09 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0832
• Residual factor for significantly intense reflections: 0.048
• Weighted residual factors for significantly intense reflections: 0.1007
• Weighted residual factors for all reflections included in the refinement: 0.1163
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No