Information card for entry 4112471

Structure parameters

• Formula: C27 H42.29 Cl N P2 Rh
• Calculated formula: C27 H42.295 Cl N P2 Rh
• Title of publication: Facile Oxidative Addition of N-C and N-H Bonds to Monovalent Rhodium and Iridium
• Authors of publication: Oleg V. Ozerov; Chengyun Guo; Vyacheslav A. Papkov; Bruce M. Foxman
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2004
• Journal volume: 126
• Pages of publication: 4792 - 4793
• a: 13.376 ± 0.004 Å
• b: 13.626 ± 0.006 Å
• c: 32.675 ± 0.011 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5955 ± 4 ų
• Cell temperature: 294 K
• Ambient diffraction temperature: 294 K
• Number of distinct elements: 6
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0955
• Residual factor for significantly intense reflections: 0.0584
• Weighted residual factors for all reflections: 0.1145
• Weighted residual factors for significantly intense reflections: 0.0609
• Weighted residual factors for all reflections included in the refinement: 0.0609
• Goodness-of-fit parameter for all reflections included in the refinement: 1.1445
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No