Information card for entry 4112489

Structure parameters

• Formula: C32.5 H25 K2 N5 O15 Sm
• Calculated formula: C32.5 H25 K2 N5 O15 Sm
• Title of publication: Nitrophenolate as a Building Block for Lanthanide Chains, Layers, and Clusters
• Authors of publication: Markus R. Bürgstein; Michael T. Gamer; Peter W. Roesky
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2004
• Journal volume: 126
• Pages of publication: 5213 - 5218
• a: 14.693 ± 0.003 Å
• b: 18.214 ± 0.008 Å
• c: 15.094 ± 0.006 Å
• α: 90°
• β: 118.97 ± 0.03°
• γ: 90°
• Cell volume: 3534 ± 2 ų
• Cell temperature: 203 ± 2 K
• Ambient diffraction temperature: 203 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0788
• Residual factor for significantly intense reflections: 0.0529
• Weighted residual factors for significantly intense reflections: 0.1324
• Weighted residual factors for all reflections included in the refinement: 0.1471
• Goodness-of-fit parameter for all reflections included in the refinement: 1.077
• Diffraction radiation wavelength: 0.56087 Å
• Diffraction radiation type: AgKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No