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Information card for entry 4112496
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Coordinates | 4112496.cif |
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Original paper (by DOI) | HTML |
Chemical name | Tetrakis(tetrahydrofuran)lithium(I) 1,1,3,3-tetrakis- [di-tert-butyl(methyl)silyl]-1,3-disila-2-gallataallene |
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Formula | C58 H122 Ga Li O4 Si6 |
Calculated formula | C58 H122 Ga Li O4 Si6 |
Title of publication | 1,3-Disila-2-gallata- and -indata allenic Anions [>SiMSi<]-.Li+ (M = Ga, In): Compounds Featuring Double Bonds between Elements of Groups 13 and 14 |
Authors of publication | Norio Nakata; Rika Izumi; Vladimir Ya. Lee; Masaaki Ichinohe; Akira Sekiguchi |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2004 |
Journal volume | 126 |
Pages of publication | 5058 - 5059 |
a | 24.229 ± 0.0012 Å |
b | 12.077 ± 0.0005 Å |
c | 24.573 ± 0.0011 Å |
α | 90° |
β | 104.763 ± 0.003° |
γ | 90° |
Cell volume | 6953 ± 0.6 Å3 |
Cell temperature | 120 ± 2 K |
Ambient diffraction temperature | 120 ± 2 K |
Number of distinct elements | 6 |
Space group number | 13 |
Hermann-Mauguin space group symbol | P 1 2/n 1 |
Hall space group symbol | -P 2yac |
Residual factor for all reflections | 0.1044 |
Residual factor for significantly intense reflections | 0.0564 |
Weighted residual factors for significantly intense reflections | 0.1332 |
Weighted residual factors for all reflections included in the refinement | 0.1516 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.926 |
Diffraction radiation wavelength | 0.7107 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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