Information card for entry 4112531

Structure parameters

• Formula: C89 H66 Ag Cl1.75 F0 O4 P4 S
• Calculated formula: C88.96 H65.73 Ag Cl1.895 O4 P4 S
• Title of publication: Enantioselective O- and N-Nitroso Aldol Synthesis of Tin Enolates. Isolation of Three BINAP-Silver Complexes and Their Role in Regio- and Enantioselectivity
• Authors of publication: Norie Momiyama; Hisashi Yamamoto
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2004
• Journal volume: 126
• Pages of publication: 5360 - 5361
• a: 11.883 ± 0.002 Å
• b: 21.427 ± 0.004 Å
• c: 28.346 ± 0.006 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 7217 ± 2 ų
• Cell temperature: 103 ± 2 K
• Ambient diffraction temperature: 103 ± 2 K
• Number of distinct elements: 8
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.048
• Residual factor for significantly intense reflections: 0.0462
• Weighted residual factors for significantly intense reflections: 0.1092
• Weighted residual factors for all reflections included in the refinement: 0.1102
• Goodness-of-fit parameter for all reflections included in the refinement: 1.152
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No