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Information card for entry 4112541
Preview
Coordinates | 4112541.cif |
---|---|
Original paper (by DOI) | HTML |
Common name | para-tolualdehyde N-tert-butyldimethylsilylhydrozone |
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Formula | C14 H24 N2 Si |
Calculated formula | C14 H24 N2 Si |
SMILES | [Si](N/N=C/c1ccc(cc1)C)(C)(C)C(C)(C)C |
Title of publication | Practical Procedures for the Preparation of N-tert-Butyldimethylsilylhydrazones and Their Use in Modified Wolff-Kishner Reductions and in the Synthesis of Vinyl Halides and gem-Dihalides |
Authors of publication | Michael E. Furrow; Andrew G. Myers |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2004 |
Journal volume | 126 |
Pages of publication | 5436 - 5445 |
a | 6.8315 ± 0.0015 Å |
b | 7.4154 ± 0.0016 Å |
c | 30.72 ± 0.007 Å |
α | 90° |
β | 93.928 ± 0.005° |
γ | 90° |
Cell volume | 1552.6 ± 0.6 Å3 |
Cell temperature | 193 ± 2 K |
Ambient diffraction temperature | 193 ± 2 K |
Number of distinct elements | 4 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.1493 |
Residual factor for significantly intense reflections | 0.0766 |
Weighted residual factors for significantly intense reflections | 0.1284 |
Weighted residual factors for all reflections included in the refinement | 0.1475 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.99 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4112541.html
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