Information card for entry 4113402

Structure parameters

• Formula: C12 H34 N2 Se2 Si2 Zn
• Calculated formula: C12 H34 N2 Se2 Si2 Zn
• Title of publication: Zinc Chalcogenolate Complexes as Capping Agents in the Synthesis of Ternary II-II'-VI Nanoclusters: Structure and Photophysical Properties of [(N,N'-tmeda)5Zn5Cd11Se13(SePh)6(thf)2]
• Authors of publication: Marty W. DeGroot; Nicholas J. Taylor; John F. Corrigan
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2003
• Journal volume: 125
• Pages of publication: 864 - 865
• a: 8.4454 ± 0.0002 Å
• b: 14.3403 ± 0.0004 Å
• c: 18.7691 ± 0.0005 Å
• α: 90°
• β: 90.112 ± 0.0011°
• γ: 90°
• Cell volume: 2273.11 ± 0.1 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1002
• Residual factor for significantly intense reflections: 0.0447
• Weighted residual factors for significantly intense reflections: 0.0808
• Weighted residual factors for all reflections included in the refinement: 0.0953
• Goodness-of-fit parameter for all reflections included in the refinement: 1.003
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No