Information card for entry 4113473

Structure parameters

• Common name: 7d(SnCl4
• Formula: C23 H46 Cl4 N6 O3 P2 Sn
• Calculated formula: C23 H44 Cl4 N6 O3 P2 Sn
• Title of publication: Understanding the Correlation of Structure and Selectivity in the Chiral-Phosphoramide-Catalyzed Enantioselective Allylation Reactions: Solution and Solid-State Structural Studies of Bisphosphoramide.SnCl4 Complexes
• Authors of publication: Scott E. Denmark; Jiping Fu
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2003
• Journal volume: 125
• Pages of publication: 2208 - 2216
• a: 14.898 ± 0.003 Å
• b: 18.01 ± 0.003 Å
• c: 12.42 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3332.4 ± 1 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 7
• Space group number: 20
• Hermann-Mauguin space group symbol: C 2 2 21
• Hall space group symbol: C 2c 2
• Residual factor for all reflections: 0.0766
• Residual factor for significantly intense reflections: 0.0398
• Weighted residual factors for significantly intense reflections: 0.0612
• Weighted residual factors for all reflections included in the refinement: 0.0679
• Goodness-of-fit parameter for all reflections included in the refinement: 0.92
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No