Information card for entry 4113557

Structure parameters

• Formula: Fe3 K9 Na0 O94.5 P2 W18
• Calculated formula: Fe3 K9 O94.5 P2 W18
• Title of publication: [(FeIII(OH2)2)3(A-α-PW9O34)2]9- on Cationic Silica Nanoparticles, a New Type of Material and Efficient Heterogeneous Catalyst for Aerobic Oxidations
• Authors of publication: Nelya M. Okun; Travis M. Anderson; Craig L. Hill
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2003
• Journal volume: 125
• Pages of publication: 3194 - 3195
• a: 40.376 ± 0.004 Å
• b: 27.904 ± 0.002 Å
• c: 31.186 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 35136 ± 5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 43
• Hermann-Mauguin space group symbol: F d d 2
• Hall space group symbol: F 2 -2d
• Residual factor for all reflections: 0.0436
• Residual factor for significantly intense reflections: 0.0419
• Weighted residual factors for significantly intense reflections: 0.0916
• Weighted residual factors for all reflections included in the refinement: 0.0924
• Goodness-of-fit parameter for all reflections included in the refinement: 1.117
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No