Information card for entry 4113571

Structure parameters

• Common name: (Dipp*GeH)~2~^.^4C~4~H~10~O
• Formula: C76 H116 Ge2 O4
• Calculated formula: C60 H76 Ge2
• Title of publication: Isomeric Forms of Divalent Heavier Group 14 Element Hydrides: Characterization of Ar'(H)GeGe(H)Ar' and Ar'(H)2GeGeAr'.PMe3 (Ar' = C6H3-2,6-Dipp2; Dipp = C6H3-2,6-Pri2)
• Authors of publication: Anne F. Richards; Andrew D. Phillips; Marilyn M. Olmstead; Philip P. Power
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2003
• Journal volume: 125
• Pages of publication: 3204 - 3205
• a: 18.3776 ± 0.0017 Å
• b: 17.7496 ± 0.0017 Å
• c: 13.0929 ± 0.0012 Å
• α: 90°
• β: 117.432 ± 0.002°
• γ: 90°
• Cell volume: 3790.6 ± 0.6 ų
• Cell temperature: 90 ± 2 K
• Ambient diffraction temperature: 90 ± 2 K
• Number of distinct elements: 4
• Space group number: 12
• Hermann-Mauguin space group symbol: C 1 2/m 1
• Hall space group symbol: -C 2y
• Residual factor for all reflections: 0.0559
• Residual factor for significantly intense reflections: 0.0495
• Weighted residual factors for significantly intense reflections: 0.1355
• Weighted residual factors for all reflections included in the refinement: 0.1398
• Goodness-of-fit parameter for all reflections included in the refinement: 1.076
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No