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Information card for entry 4113865
Preview
Coordinates | 4113865.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C16 H48 P4 Ru Si |
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Calculated formula | C16 H48 P4 Ru Si |
SMILES | [Ru]([P](C)(C)C)([P](C)(C)C)([P](C)(C)C)([P](C)(C)C)([Si](C)(C)C)C |
Title of publication | Synthesis and Reactivity of Silyl Ruthenium Complexes: The Importance of Trans Effects in C-H Activation, Si-C Bond Formation, and Dehydrogenative Coupling of Silanes |
Authors of publication | Vladimir K. Dioumaev; Leo J. Procopio; Patrick J. Carroll; Donald H. Berry |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2003 |
Journal volume | 125 |
Pages of publication | 8043 - 8058 |
a | 15.2642 ± 0.0002 Å |
b | 10.9388 ± 0.0001 Å |
c | 31.0714 ± 0.0004 Å |
α | 90° |
β | 103.982 ± 0.001° |
γ | 90° |
Cell volume | 5034.34 ± 0.11 Å3 |
Cell temperature | 200 ± 2 K |
Ambient diffraction temperature | 200 ± 2 K |
Number of distinct elements | 5 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.0653 |
Residual factor for significantly intense reflections | 0.0554 |
Weighted residual factors for all reflections | 0.1295 |
Weighted residual factors for significantly intense reflections | 0.1239 |
Goodness-of-fit parameter for all reflections | 1.215 |
Goodness-of-fit parameter for significantly intense reflections | 1.238 |
Diffraction radiation wavelength | 0.71069 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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