Information card for entry 4113986

Structure parameters

• Formula: C16.5 H37 Fe N O P4
• Calculated formula: C16.5 H37 Fe N O P4
• Title of publication: Synthesis of a First-Row Transition Metal Parent Amido Complex and Carbon Monoxide Insertion into the Amide N-H Bond
• Authors of publication: Daniel J. Fox; Robert G. Bergman
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2003
• Journal volume: 125
• Pages of publication: 8984 - 8985
• a: 29.11 ± 0.003 Å
• b: 14.188 ± 0.002 Å
• c: 11.25 ± 0.001 Å
• α: 90°
• β: 98.222 ± 0.002°
• γ: 90°
• Cell volume: 4598.6 ± 0.9 ų
• Cell temperature: 158.2 K
• Ambient diffraction temperature: 158.2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.08
• Residual factor for significantly intense reflections: 0.0371
• Weighted residual factors for significantly intense reflections: 0.0419
• Weighted residual factors for all reflections included in the refinement: 0.0475
• Goodness-of-fit parameter for all reflections included in the refinement: 1.31
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No