Information card for entry 4114114

Structure parameters

• Common name: polyoxovanadogermanate
• Formula: C8 H28 Ge4 N4 O28 V7
• Calculated formula: C8 H28 Ge4 N4 O28 V7
• Title of publication: The First Framework Solid Composed of Vanadosilicate Clusters
• Authors of publication: Akhilesh Tripathi; Timothy Hughbanks; Abraham Clearfield
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2003
• Journal volume: 125
• Pages of publication: 10528 - 10529
• a: 15.588 ± 0.002 Å
• b: 15.588 ± 0.002 Å
• c: 16.268 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3952.9 ± 1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 86
• Hermann-Mauguin space group symbol: P 42/n :2
• Hall space group symbol: -P 4bc
• Residual factor for all reflections: 0.0677
• Residual factor for significantly intense reflections: 0.0453
• Weighted residual factors for significantly intense reflections: 0.1265
• Weighted residual factors for all reflections included in the refinement: 0.1358
• Goodness-of-fit parameter for all reflections included in the refinement: 1.079
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No