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Information card for entry 4114157
Preview
Coordinates | 4114157.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C10 H50 K9 N4 Na4 O85 P2 Ru W19 |
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Calculated formula | C10 K9 N4 Na4 O85 P2 Ru W19 |
SMILES | [W]1234(=O)=[O][Ru]56([O]=[W]78(O2)(=O)O[W]29(O[W]%10%11(O[W]%12%13%14(O[W]%15(O1)(=O)(O[W]1%16(O3)(=O)O[W]3(O%12)(O%10)(=O)O[W](O2)(O7)(O1)(=O)[O]%163P(=[O]%14%15)([O]9%11)[O]48)O[W]1(=O)(=O)(O%13)O[W]234(=O)O[W]78(=O)(=[O]6)O[W]69(=O)(=[O]5)O[W]5%10(=O)(=O)O[W]%11%12(=O)(=O)O[W]%13(=O)(O2)(O[W]2%14(=O)(O%11)O[W]%11(=O)(O6)(O5)O[W](=O)(O7)(O3)(O2)[O@]%14%11P(=[O]89)([O]%10%12)[O]4%13)O1)=O)(=O)=O)(=O)=O)(=C1N(CCN1C)C)=C1N(CCN1C)C.[K+].[K+].[K+].[K+].[K+].[K+].[K+].[K+].O.[K+].[Na+].[Na+].[Na+].[Na+].O.O.O.O.O.O.O.O.O.O.O.O.O.O |
Title of publication | Synthesis and Characterization of the First Carbene Derivative of a Polyoxometalate |
Authors of publication | Vincent Artero; Anna Proust; Patrick Herson; Françoise Villain; Christophe Cartier dit Moulin; Pierre Gouzerh |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2003 |
Journal volume | 125 |
Pages of publication | 11156 - 11157 |
a | 14.82 ± 0.003 Å |
b | 17.064 ± 0.005 Å |
c | 25.011 ± 0.005 Å |
α | 99.03 ± 0.03° |
β | 106.56 ± 0.02° |
γ | 108.06 ± 0.02° |
Cell volume | 5551 ± 3 Å3 |
Cell temperature | 295 ± 2 K |
Ambient diffraction temperature | 298 K |
Number of distinct elements | 9 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for significantly intense reflections | 0.067 |
Weighted residual factors for significantly intense reflections | 0.0792 |
Goodness-of-fit parameter for significantly intense reflections | 1.0738 |
Diffraction radiation wavelength | 0.71069 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4114157.html
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