Information card for entry 4114191

Structure parameters

• Common name: (Dipp*Sn)2K(THF)6.2THF
• Formula: C88 H130 K O8 Sn2
• Calculated formula: C88 H130 K O8 Sn2
• Title of publication: Germanium and Tin Analogues of Alkynes and Their Reduction Products
• Authors of publication: Lihung Pu; Andrew D. Phillips; Anne F. Richards; Matthias Stender; Richard S. Simons; Marilyn M. Olmstead; Philip P. Power
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2003
• Journal volume: 125
• Pages of publication: 11626 - 11636
• a: 17.433 ± 0.002 Å
• b: 18.014 ± 0.003 Å
• c: 14.475 ± 0.0018 Å
• α: 90°
• β: 96.551 ± 0.004°
• γ: 90°
• Cell volume: 4516 ± 1.1 ų
• Cell temperature: 143 ± 2 K
• Ambient diffraction temperature: 143 ± 2 K
• Number of distinct elements: 5
• Space group number: 12
• Hermann-Mauguin space group symbol: C 1 2/m 1
• Hall space group symbol: -C 2y
• Residual factor for all reflections: 0.0705
• Residual factor for significantly intense reflections: 0.0546
• Weighted residual factors for significantly intense reflections: 0.1542
• Weighted residual factors for all reflections included in the refinement: 0.175
• Goodness-of-fit parameter for all reflections included in the refinement: 1.154
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No