Information card for entry 4114193

Structure parameters

• Common name: (Dipp*SnK)2.1.5C6H6
• Formula: C78 H92 K2 Sn2
• Calculated formula: C79 H92 K2 Sn2
• Title of publication: Germanium and Tin Analogues of Alkynes and Their Reduction Products
• Authors of publication: Lihung Pu; Andrew D. Phillips; Anne F. Richards; Matthias Stender; Richard S. Simons; Marilyn M. Olmstead; Philip P. Power
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2003
• Journal volume: 125
• Pages of publication: 11626 - 11636
• a: 26.268 ± 0.002 Å
• b: 18.7851 ± 0.0016 Å
• c: 15.0562 ± 0.0013 Å
• α: 90°
• β: 111.697 ± 0.002°
• γ: 90°
• Cell volume: 6903.1 ± 1 ų
• Cell temperature: 90 ± 2 K
• Ambient diffraction temperature: 90 ± 2 K
• Number of distinct elements: 4
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0284
• Residual factor for significantly intense reflections: 0.0242
• Weighted residual factors for significantly intense reflections: 0.0586
• Weighted residual factors for all reflections included in the refinement: 0.0617
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No