Information card for entry 4114195

Structure parameters

• Formula: C17 H36 Cl18 N W6
• Calculated formula: C17 Cl18 N W6
• Title of publication: New Routes to Transition Metal-Carbido Species: Synthesis and Characterization of the Carbon-Centered Trigonal Prismatic Clusters [W6CCl18]n- (n= 1, 2, 3)
• Authors of publication: Eric J. Welch; Nathan R. M. Crawford; Robert G. Bergman; Jeffrey R. Long
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2003
• Journal volume: 125
• Pages of publication: 11464 - 11465
• a: 12.4658 ± 0.0005 Å
• b: 13.2168 ± 0.0005 Å
• c: 13.6449 ± 0.0005 Å
• α: 99.757 ± 0.002°
• β: 113.24 ± 0.001°
• γ: 92.073 ± 0.002°
• Cell volume: 2022.59 ± 0.14 ų
• Cell temperature: 113 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0742
• Residual factor for significantly intense reflections: 0.0492
• Weighted residual factors for all reflections: 0.1347
• Weighted residual factors for significantly intense reflections: 0.1193
• Goodness-of-fit parameter for all reflections: 1.018
• Goodness-of-fit parameter for significantly intense reflections: 1.063
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No