Information card for entry 4114267

Structure parameters

• Chemical name: Tris(trimethylsilyl)tetrahedranyllithium (N,N,N',N'-tetramethyletylenediamine)
• Formula: C22 H51 Li N3 Si3
• Calculated formula: C22 H51 Li N3 Si3
• Title of publication: Tetrahedranyllithium: Synthesis, Characterization, and Reactivity
• Authors of publication: Akira Sekiguchi; Masanobu Tanaka
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2003
• Journal volume: 125
• Pages of publication: 12684 - 12685
• a: 9.139 ± 0.0002 Å
• b: 15.139 ± 0.0005 Å
• c: 22.115 ± 0.0006 Å
• α: 90°
• β: 94.278 ± 0.002°
• γ: 90°
• Cell volume: 3051.2 ± 0.15 ų
• Cell temperature: 120 K
• Ambient diffraction temperature: 120 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0426
• Residual factor for significantly intense reflections: 0.0368
• Weighted residual factors for significantly intense reflections: 0.1012
• Weighted residual factors for all reflections included in the refinement: 0.1054
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No