Information card for entry 4114296

Structure parameters

• Formula: C12 H25 Br Si Te
• Calculated formula: C12 H25 Br Si Te
• SMILES: [Br-].[Te+]1([C@@H](CC[C@H]1C)C)C/C=C/[Si](C)(C)C
• Title of publication: Controllable Diastereoselective Cyclopropanation. Enantioselective Synthesis of Vinylcyclopropanes via Chiral Telluronium Ylides
• Authors of publication: Wei-Wei Liao; Kai Li; Yong Tang
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2003
• Journal volume: 125
• Pages of publication: 13030 - 13031
• a: 11.8162 ± 0.001 Å
• b: 14.1277 ± 0.0011 Å
• c: 10.3477 ± 0.0008 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1727.4 ± 0.2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 18
• Hermann-Mauguin space group symbol: P 21 21 2
• Hall space group symbol: P 2 2ab
• Residual factor for all reflections: 0.0646
• Residual factor for significantly intense reflections: 0.0392
• Weighted residual factors for significantly intense reflections: 0.0667
• Weighted residual factors for all reflections included in the refinement: 0.072
• Goodness-of-fit parameter for all reflections included in the refinement: 0.812
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No