Information card for entry 4114353

Structure parameters

• Chemical name: (K-crypt)4[Ph2Sb-Ge9-Ge9-SbPh2].2.5en
• Formula: C101 H184 Ge18 K4 N13 O24 Sb2
• Calculated formula: C101 H184.05 Ge18 K4 N13 O24 Sb2
• Title of publication: Derivatization of Deltahedral Zintl Ions by Nucleophilic Addition: [Ph-Ge9-SbPh2]2-and [Ph2Sb-Ge9-Ge9-SbPh2]4-
• Authors of publication: Angel Ugrinov; Slavi C. Sevov
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2003
• Journal volume: 125
• Pages of publication: 14059 - 14064
• a: 14.333 ± 0.005 Å
• b: 26.108 ± 0.008 Å
• c: 38.643 ± 0.014 Å
• α: 80.472 ± 0.007°
• β: 82.169 ± 0.006°
• γ: 84.332 ± 0.008°
• Cell volume: 14085 ± 8 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1734
• Residual factor for significantly intense reflections: 0.084
• Weighted residual factors for significantly intense reflections: 0.1928
• Weighted residual factors for all reflections included in the refinement: 0.2404
• Goodness-of-fit parameter for all reflections included in the refinement: 1.002
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No