Information card for entry 4114358

Structure parameters

• Chemical name: (Rb-crypt)2Rb4(Ge9)(Ge9).7en
• Formula: C24 H34 Ge9 N9 O6 Rb3
• Calculated formula: C24 H34 Ge9 N9 O6 Rb3
• Title of publication: Derivatization of Deltahedral Zintl Ions by Nucleophilic Addition: [Ph-Ge9-SbPh2]2-and [Ph2Sb-Ge9-Ge9-SbPh2]4-
• Authors of publication: Angel Ugrinov; Slavi C. Sevov
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2003
• Journal volume: 125
• Pages of publication: 14059 - 14064
• a: 10.138 ± 0.003 Å
• b: 13.881 ± 0.002 Å
• c: 19.311 ± 0.004 Å
• α: 76.76 ± 0.01°
• β: 80.9 ± 0.02°
• γ: 78.6 ± 0.01°
• Cell volume: 2574.9 ± 1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.2263
• Residual factor for significantly intense reflections: 0.0948
• Weighted residual factors for significantly intense reflections: 0.209
• Weighted residual factors for all reflections included in the refinement: 0.2541
• Goodness-of-fit parameter for all reflections included in the refinement: 0.963
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No