Information card for entry 4114562

Structure parameters

• Formula: C60 H94 K2 O16 Si2
• Calculated formula: C60 H94 K2 O16 Si2
• Title of publication: Structure and Chemistry of 1-Silafluorenyl Dianion, Its Derivatives, and an Organosilicon Diradical Dianion
• Authors of publication: Yuxia Liu; Thomas C. Stringfellow; David Ballweg; Ilia A. Guzei; Robert West
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2002
• Journal volume: 124
• Pages of publication: 49 - 57
• a: 9.499 ± 0.003 Å
• b: 12.856 ± 0.004 Å
• c: 14.846 ± 0.004 Å
• α: 72.274 ± 0.004°
• β: 76.17 ± 0.005°
• γ: 68.932 ± 0.004°
• Cell volume: 1594.3 ± 0.8 ų
• Cell temperature: 133 ± 2 K
• Ambient diffraction temperature: 133 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.104
• Residual factor for significantly intense reflections: 0.0703
• Weighted residual factors for significantly intense reflections: 0.1722
• Weighted residual factors for all reflections included in the refinement: 0.1946
• Goodness-of-fit parameter for all reflections included in the refinement: 1.071
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No