Information card for entry 4114565

Structure parameters

• Formula: C36 H57.33 K2 O10 Si
• Calculated formula: C32 H48 K2 O10 Si
• Title of publication: Structure and Chemistry of 1-Silafluorenyl Dianion, Its Derivatives, and an Organosilicon Diradical Dianion
• Authors of publication: Yuxia Liu; Thomas C. Stringfellow; David Ballweg; Ilia A. Guzei; Robert West
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2002
• Journal volume: 124
• Pages of publication: 49 - 57
• a: 10.5459 ± 0.0009 Å
• b: 15.9281 ± 0.0012 Å
• c: 17.8197 ± 0.0015 Å
• α: 95.02 ± 0.002°
• β: 98.726 ± 0.002°
• γ: 96.053 ± 0.002°
• Cell volume: 2925.8 ± 0.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1203
• Residual factor for significantly intense reflections: 0.063
• Weighted residual factors for significantly intense reflections: 0.169
• Weighted residual factors for all reflections included in the refinement: 0.1963
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No