Information card for entry 4114661

Structure parameters

• Formula: C59 H122 Mo2 N18 O4
• Calculated formula: C59 H102 Mo2 N18 O4
• Title of publication: Cyanide-Limited Complexation of Molybdenum(III): Synthesis of Octahedral [Mo(CN)6]3- and Cyano-Bridged [Mo2(CN)11]5-
• Authors of publication: Laurance G. Beauvais; Jeffrey R. Long
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2002
• Journal volume: 124
• Pages of publication: 2110 - 2111
• a: 10.6037 ± 0.0002 Å
• b: 11.9623 ± 0.0003 Å
• c: 15.2316 ± 0.0001 Å
• α: 96.627 ± 0.001°
• β: 107.77 ± 0.001°
• γ: 94.86 ± 0.001°
• Cell volume: 1812.82 ± 0.06 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0768
• Residual factor for significantly intense reflections: 0.0604
• Weighted residual factors for all reflections: 0.184
• Weighted residual factors for significantly intense reflections: 0.1642
• Goodness-of-fit parameter for all reflections: 1.034
• Goodness-of-fit parameter for significantly intense reflections: 1.085
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No