Crystallography Open Database

Information card for entry 4114679

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Coordinates	4114679.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C17 H35 Br O S Si
Calculated formula	C34 H70 Br2 O2 S2 Si2
Title of publication	A Novel Chiral Sulfonium Yilde: Highly Enantioselective Synthesis of Vinylcyclopropanes
Authors of publication	Song Ye; Zheng-Zheng Huang; Chun-An Xia; Yong Tang; Li-Xin Dai
Journal of publication	Journal of the American Chemical Society
Year of publication	2002
Journal volume	124
Pages of publication	2432 - 2433
a	7.621 ± 0.002 Å
b	9.817 ± 0.002 Å
c	14.663 ± 0.004 Å
α	90°
β	91.74 ± 0.03°
γ	90°
Cell volume	1096.5 ± 0.5 Å³
Cell temperature	20 K
Ambient diffraction temperature	20 K
Number of distinct elements	6
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for significantly intense reflections	0.062
Weighted residual factors for significantly intense reflections	0.069
Goodness-of-fit parameter for significantly intense reflections	2.44
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKalpha
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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