Information card for entry 4114713

Structure parameters

• Formula: C29 H44 Fe O P4
• Calculated formula: C29 H44 Fe O P4
• Title of publication: Acetylide-Bridged Organometallic Oligomers via the Photochemical Metathesis of Methyl-Iron(II) Complexes
• Authors of publication: Leslie D. Field; Anthony J. Turnbull; Peter Turner
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2002
• Journal volume: 124
• Pages of publication: 3692 - 3702
• a: 9.108 ± 0.002 Å
• b: 18.09 ± 0.003 Å
• c: 9.526 ± 0.001 Å
• α: 90°
• β: 94.42 ± 0.01°
• γ: 90°
• Cell volume: 1564.9 ± 0.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 294 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/a 1
• Hall space group symbol: -P 2yab
• Residual factor for all reflections: 0.1371
• Residual factor for significantly intense reflections: 0.0658
• Weighted residual factors for significantly intense reflections: 0.1803
• Weighted residual factors for all reflections included in the refinement: 0.1962
• Goodness-of-fit parameter for all reflections included in the refinement: 1.498
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No