Crystallography Open Database

Information card for entry 4114752

Preview

Coordinates	4114752.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C112 H190 K4 N12 O24 P2 Pt4 Sn18
Calculated formula	C112 H190 K4 N12 O24 P2 Pt4 Sn18
Title of publication	The [Sn9Pt2(PPh3)]2- and [Sn9Ni2(CO)]3- Complexes: Two Markedly Different Sn9M2L Transition Metal Zintl Ion Clusters and Their Dynamic Behavior
Authors of publication	Banu Kesanli; James Fettinger; Donna R. Gardner; Bryan Eichhorn
Journal of publication	Journal of the American Chemical Society
Year of publication	2002
Journal volume	124
Pages of publication	4779 - 4786
a	13.1703 ± 0.0006 Å
b	13.312 ± 0.0006 Å
c	24.3236 ± 0.001 Å
α	79.445 ± 0.001°
β	76.067 ± 0.001°
γ	83.726 ± 0.001°
Cell volume	4059.5 ± 0.3 Å³
Cell temperature	193 ± 2 K
Ambient diffraction temperature	193 ± 2 K
Number of distinct elements	8
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.079
Residual factor for significantly intense reflections	0.0398
Weighted residual factors for significantly intense reflections	0.0684
Weighted residual factors for all reflections included in the refinement	0.0819
Goodness-of-fit parameter for all reflections included in the refinement	1.012
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4114752.html