Information card for entry 4114754

Structure parameters

• Formula: C528 H988 K24 N64 Ni16 O152 P4 Sn72
• Calculated formula: C528 H988 K24 N64 Ni16 O152 P4 Sn72
• Title of publication: The [Sn9Pt2(PPh3)]2- and [Sn9Ni2(CO)]3- Complexes: Two Markedly Different Sn9M2L Transition Metal Zintl Ion Clusters and Their Dynamic Behavior
• Authors of publication: Banu Kesanli; James Fettinger; Donna R. Gardner; Bryan Eichhorn
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2002
• Journal volume: 124
• Pages of publication: 4779 - 4786
• a: 31.197 ± 0.001 Å
• b: 23.8741 ± 0.0008 Å
• c: 27.9617 ± 0.0009 Å
• α: 90°
• β: 113.047 ± 0.001°
• γ: 90°
• Cell volume: 19163.6 ± 1.1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0849
• Residual factor for significantly intense reflections: 0.0513
• Weighted residual factors for significantly intense reflections: 0.1403
• Weighted residual factors for all reflections included in the refinement: 0.1558
• Goodness-of-fit parameter for all reflections included in the refinement: 1.059
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No