Crystallography Open Database

Information card for entry 4114866

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Coordinates	4114866.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C33.5 H52 Cl4 P2 Rh
Calculated formula	C33.5 H52 Cl4 P2 Rh
Title of publication	Unusual Pathways for Metal-Assisted C-C and C-P Coupling Reactions Using Allenylidenerhodium Complexes as Precursors
Authors of publication	Helmut Werner; Ralf Wiedemann; Matthias Laubender; Bettina Windmüller; Paul Steinert; Olaf Gevert; Justin Wolf
Journal of publication	Journal of the American Chemical Society
Year of publication	2002
Journal volume	124
Pages of publication	6966 - 6980
a	9.463 ± 0.004 Å
b	11.369 ± 0.005 Å
c	17.936 ± 0.009 Å
α	92 ± 0.03°
β	97.9 ± 0.02°
γ	108.25 ± 0.02°
Cell volume	1808.9 ± 1.5 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0481
Residual factor for significantly intense reflections	0.0317
Weighted residual factors for all reflections	0.0858
Weighted residual factors for significantly intense reflections	0.0791
Goodness-of-fit parameter for all reflections	1.057
Goodness-of-fit parameter for significantly intense reflections	1.068
Diffraction radiation wavelength	0.7093 Å
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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