Information card for entry 4114908

Structure parameters

• Formula: C20 H24 Cl3 O8 P4 Rh
• Calculated formula: C19.994 H24 Cl3 O8 P4 Rh
• Title of publication: Exceptional Kinetic Propensity of Hydroxymethyl Phosphanes toward Rh(III) Stabilization in Water
• Authors of publication: Kannan Raghuraman; Nagavarakishore Pillarsetty; Wynn A. Volkert; Charles Barnes; Silvia Jurisson; Kattesh V. Katti
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2002
• Journal volume: 124
• Pages of publication: 7276 - 7277
• a: 8.3195 ± 0.0012 Å
• b: 9.8962 ± 0.0014 Å
• c: 18.175 ± 0.003 Å
• α: 97.034 ± 0.002°
• β: 92.03 ± 0.003°
• γ: 113.688 ± 0.002°
• Cell volume: 1354.1 ± 0.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0651
• Residual factor for significantly intense reflections: 0.0586
• Weighted residual factors for significantly intense reflections: 0.166
• Weighted residual factors for all reflections included in the refinement: 0.169
• Goodness-of-fit parameter for all reflections included in the refinement: 1.067
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No