Crystallography Open Database

Information card for entry 4115011

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Coordinates	4115011.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C48 H144 Cl9 N24 O24 Ru4
Calculated formula	C48 H96 Cl9.12 N24 O24.02 Ru4
Title of publication	[(Cyclen)4Ru4(pz)4]9+: A Creutz-Taube Square
Authors of publication	Victor C. Lau; Louise A. Berben; Jeffrey R. Long
Journal of publication	Journal of the American Chemical Society
Year of publication	2002
Journal volume	124
Pages of publication	9042 - 9043
a	8.66 ± 0.006 Å
b	38.787 ± 0.026 Å
c	56.28 ± 0.037 Å
α	90°
β	90°
γ	90°
Cell volume	18904 ± 2 Å³
Cell temperature	129 ± 2 K
Ambient diffraction temperature	129 ± 2 K
Number of distinct elements	6
Space group number	70
Hermann-Mauguin space group symbol	F d d d :2
Hall space group symbol	-F 2uv 2vw
Residual factor for all reflections	0.1658
Residual factor for significantly intense reflections	0.0794
Weighted residual factors for all reflections	0.2486
Weighted residual factors for significantly intense reflections	0.1908
Goodness-of-fit parameter for all reflections	1.019
Goodness-of-fit parameter for significantly intense reflections	1.186
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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