Information card for entry 4115142

Structure parameters

• Chemical name: (Rb-2,2,2-crypt)6[Ge9=Ge9=Ge9].3en
• Formula: C114 H240 Ge27 N18 O36 Rb6
• Calculated formula: C114 H240.06 Ge27 N18 O36 Rb6
• Title of publication: [Ge9Ge9Ge9]6-: A Linear Trimer of 27 Germanium Atoms
• Authors of publication: Angel Ugrinov; Slavi C. Sevov
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2002
• Journal volume: 124
• Pages of publication: 10990 - 10991
• a: 15.246 ± 0.002 Å
• b: 47.223 ± 0.007 Å
• c: 26.657 ± 0.004 Å
• α: 90°
• β: 98.373 ± 0.003°
• γ: 90°
• Cell volume: 18987 ± 5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1448
• Residual factor for significantly intense reflections: 0.0728
• Weighted residual factors for significantly intense reflections: 0.1878
• Weighted residual factors for all reflections included in the refinement: 0.2274
• Goodness-of-fit parameter for all reflections included in the refinement: 1.017
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No