Information card for entry 4115172

Structure parameters

• Formula: C16 H31 Ge Li O Si2
• Calculated formula: C16 H39 Ge Li O Si2
• Title of publication: Sila-metalation Route to Hydrido(trialkylsilyl)silyllithiums
• Authors of publication: Takeaki Iwamoto; Junichiro Okita; Chizuko Kabuto; Mitsuo Kira
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2002
• Journal volume: 124
• Pages of publication: 11604 - 11605
• a: 11.88 ± 0.002 Å
• b: 15.941 ± 0.002 Å
• c: 12.802 ± 0.001 Å
• α: 90°
• β: 107.25 ± 0.0009°
• γ: 90°
• Cell volume: 2315.4 ± 0.5 ų
• Cell temperature: 123.2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for significantly intense reflections: 0.0448
• Weighted residual factors for all reflections included in the refinement: 0.1217
• Goodness-of-fit parameter for all reflections included in the refinement: 0.906
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No