Information card for entry 4115246

Structure parameters

• Formula: C33 H61 F9 N6 O22 P4 Ru2 S5
• Calculated formula: C33.04 H37 F9 N6 O22 P4 Ru2 S5
• Title of publication: Dehydration Reaction of Hydroxyl Substituted Alkenes and Alkynes on the Ru2S2 Complex
• Authors of publication: Kazuko Matsumoto; Yoshihiro Moriya; Hiroyasu Sugiyama; Md. Munkir Hossain; Yong-Shou Lin
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2002
• Journal volume: 124
• Pages of publication: 13106 - 13113
• a: 12.5969 ± 0.0011 Å
• b: 13.7742 ± 0.0012 Å
• c: 18.7252 ± 0.0017 Å
• α: 90.962 ± 0.002°
• β: 90.459 ± 0.002°
• γ: 107.41 ± 0.002°
• Cell volume: 3099.5 ± 0.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0991
• Residual factor for significantly intense reflections: 0.0871
• Weighted residual factors for significantly intense reflections: 0.2122
• Weighted residual factors for all reflections included in the refinement: 0.2226
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No