Information card for entry 4115345

Structure parameters

• Formula: C44 H47 Mo2 O4 P
• Calculated formula: C44 H47 Mo2 O4 P
• Title of publication: High Yield Synthesis and Reactivity of a Phosphinidene Bridged Dimolybdenum Complex
• Authors of publication: M. Esther García; Víctor Riera; Miguel A. Ruiz; David Sáez; Jacqueline Vaissermann; John C. Jeffery
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2002
• Journal volume: 124
• Pages of publication: 14304 - 14305
• a: 10.107 ± 0.0012 Å
• b: 24.32 ± 0.003 Å
• c: 16.839 ± 0.002 Å
• α: 90°
• β: 98.244 ± 0.017°
• γ: 90°
• Cell volume: 4096.3 ± 0.9 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0482
• Residual factor for significantly intense reflections: 0.0368
• Weighted residual factors for significantly intense reflections: 0.0952
• Weighted residual factors for all reflections included in the refinement: 0.0981
• Goodness-of-fit parameter for all reflections included in the refinement: 0.955
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No