Information card for entry 4115384

Structure parameters

• Formula: C130 H325 Cu70 O P21 Se35
• Calculated formula: C130 Cu70.01 O P21 Se35
• Title of publication: Cluster Synthesis via Ligand-Arrested Solid Growth: Triethylphosphine-Capped Fragments of Binary Metal Chalcogenides
• Authors of publication: Nathan R. M. Crawford; Allan G. Hee; Jeffrey R. Long
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2002
• Journal volume: 124
• Pages of publication: 14842 - 14843
• a: 25.6986 ± 0.0015 Å
• b: 35.504 ± 0.003 Å
• c: 29.214 ± 0.002 Å
• α: 90°
• β: 100.573 ± 0.003°
• γ: 90°
• Cell volume: 26202 ± 3 ų
• Cell temperature: 147 ± 2 K
• Ambient diffraction temperature: 147 ± 2 K
• Number of distinct elements: 6
• Space group number: 7
• Hermann-Mauguin space group symbol: P 1 c 1
• Hall space group symbol: P -2yc
• Residual factor for all reflections: 0.3223
• Residual factor for significantly intense reflections: 0.1581
• Weighted residual factors for significantly intense reflections: 0.34
• Weighted residual factors for all reflections included in the refinement: 0.4339
• Goodness-of-fit parameter for all reflections included in the refinement: 1.313
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No