Information card for entry 4115418

Structure parameters

• Formula: C32 H38 F2 N2 Si3
• Calculated formula: C32 H38 F2 N2 Si3
• SMILES: [Si@]1(N([Si](F)(F)N1[Si](C(C)(C)C)(c1ccccc1)c1ccccc1)c1ccccc1)(C(C)(C)C)c1ccccc1
• Title of publication: Silyl Group Insertion into the N-N Bond: Experimental and Quantum Chemical Results
• Authors of publication: Eike Gellermann; Uwe Klingebiel; Mathias Noltemeyer; Stefan Schmatz
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2001
• Journal volume: 123
• Pages of publication: 378 - 382
• a: 8.4817 ± 0.0011 Å
• b: 11.1925 ± 0.0015 Å
• c: 16.342 ± 0.003 Å
• α: 90°
• β: 98.482 ± 0.012°
• γ: 90°
• Cell volume: 1534.4 ± 0.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0601
• Residual factor for significantly intense reflections: 0.0497
• Weighted residual factors for all reflections: 0.1288
• Weighted residual factors for significantly intense reflections: 0.1166
• Goodness-of-fit parameter for all reflections: 1.035
• Goodness-of-fit parameter for significantly intense reflections: 1.026
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No