Information card for entry 4115433

Structure parameters

• Formula: C16 H41 Ge N Si4
• Calculated formula: C16 H41 Ge N Si4
• Title of publication: Intermolecular C-H Insertions and Cyclization Reactions Involving a Stable Germylene
• Authors of publication: Karla A. Miller; Thomas W. Watson; John E. Bender; Mark M. Banaszak Holl; Jeff W. Kampf
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2001
• Journal volume: 123
• Pages of publication: 982 - 983
• a: 14.2877 ± 0.0002 Å
• b: 21.2552 ± 0.0004 Å
• c: 8.2422 ± 0.0002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2503.06 ± 0.08 ų
• Cell temperature: 158 ± 2 K
• Ambient diffraction temperature: 158 ± 2 K
• Number of distinct elements: 5
• Space group number: 41
• Hermann-Mauguin space group symbol: A b a 2
• Hall space group symbol: A 2 -2ab
• Residual factor for all reflections: 0.0635
• Residual factor for significantly intense reflections: 0.0502
• Weighted residual factors for significantly intense reflections: 0.1174
• Weighted residual factors for all reflections included in the refinement: 0.1268
• Goodness-of-fit parameter for all reflections included in the refinement: 1.07
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No