Information card for entry 4115444

Structure parameters

• Formula: C37 H18 Ag24 B2 F53 N3 O39
• Calculated formula: C36 Ag24 B2 F53 N3.86 O39
• Title of publication: Elliptic Column Consolidated by Acetylide Dianion, Cyanide, and Trifluoroacetate in a Novel Quadruple Salt of Silver(I)
• Authors of publication: Quan-Ming Wang; Thomas C. W. Mak
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2001
• Journal volume: 123
• Pages of publication: 1501 - 1502
• a: 26.372 ± 0.003 Å
• b: 25.257 ± 0.003 Å
• c: 15.9775 ± 0.0016 Å
• α: 90°
• β: 103.804 ± 0.002°
• γ: 90°
• Cell volume: 10335 ± 2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1235
• Residual factor for significantly intense reflections: 0.0657
• Weighted residual factors for significantly intense reflections: 0.1996
• Weighted residual factors for all reflections included in the refinement: 0.2311
• Goodness-of-fit parameter for all reflections included in the refinement: 0.953
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No