Information card for entry 4115669

Structure parameters

• Formula: C34 H60 Li N4 O Si Ta
• Calculated formula: C34 H60 Li N4 O Si Ta
• Title of publication: Reactivity of a Tantalum-Lithium Alkylidene Supported by an Anionic Triazacyclononane Ligand
• Authors of publication: Joseph A. R. Schmidt; John Arnold
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2001
• Journal volume: 123
• Pages of publication: 8424 - 8425
• a: 11.5447 ± 0.0002 Å
• b: 13.0903 ± 0.0001 Å
• c: 13.6676 ± 0.0002 Å
• α: 63.756 ± 0.001°
• β: 84.93 ± 0.001°
• γ: 77.214 ± 0.001°
• Cell volume: 1806.54 ± 0.05 ų
• Cell temperature: 168.2 K
• Ambient diffraction temperature: 168.2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0264
• Residual factor for significantly intense reflections: 0.0209
• Weighted residual factors for all reflections: 0.0963
• Weighted residual factors for significantly intense reflections: 0.0696
• Goodness-of-fit parameter for significantly intense reflections: 2.736
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No