Information card for entry 4115671

Structure parameters

• Formula: C44 H86 N4 O Rh Si2 Ta
• Calculated formula: C44 H86 N4 O Rh Si2 Ta
• Title of publication: Reactivity of a Tantalum-Lithium Alkylidene Supported by an Anionic Triazacyclononane Ligand
• Authors of publication: Joseph A. R. Schmidt; John Arnold
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2001
• Journal volume: 123
• Pages of publication: 8424 - 8425
• a: 11.005 ± 0.0002 Å
• b: 13.5425 ± 0.0003 Å
• c: 17.5754 ± 0.0004 Å
• α: 108.303 ± 0.001°
• β: 93.722 ± 0.001°
• γ: 95.154 ± 0.001°
• Cell volume: 2464.74 ± 0.09 ų
• Cell temperature: 149.2 K
• Ambient diffraction temperature: 149.2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0557
• Residual factor for significantly intense reflections: 0.0404
• Weighted residual factors for all reflections: 0.0524
• Weighted residual factors for significantly intense reflections: 0.0444
• Goodness-of-fit parameter for significantly intense reflections: 1.436
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No