Information card for entry 4115694

Structure parameters

• Formula: C37 H29 P Si
• Calculated formula: C37 H29 P Si
• Title of publication: Phosphonium Sila-ylide: Reaction Pathway Different from Ammonium Sila-ylide but Similar to Phosphonium Ylide
• Authors of publication: Akio Toshimitsu; Tomoyuki Saeki; Kohei Tamao
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2001
• Journal volume: 123
• Pages of publication: 9210 - 9211
• a: 16.667 ± 0.001 Å
• b: 9.2935 ± 0.0006 Å
• c: 17.903 ± 0.001 Å
• α: 90°
• β: 94.538 ± 0.003°
• γ: 90°
• Cell volume: 2764.4 ± 0.3 ų
• Cell temperature: 173.2 K
• Ambient diffraction temperature: 173.2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0654
• Residual factor for significantly intense reflections: 0.0654
• Weighted residual factors for significantly intense reflections: 0.0848
• Weighted residual factors for all reflections included in the refinement: 0.0848
• Goodness-of-fit parameter for all reflections included in the refinement: 1.213
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No