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Information card for entry 4115704
Preview
Coordinates | 4115704.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C21 H21 I N2 O2 |
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Calculated formula | C21 H21 I N2 O2 |
Title of publication | Approaches to the Synthesis of (\±)-Strychnine via the Cobalt-Mediated [2 + 2 + 2] Cycloaddition: Rapid Assembly of a Classic Framework |
Authors of publication | Michael J. Eichberg; Rosa L. Dorta; Douglas B. Grotjahn; Kai Lamottke; Martin Schmidt; K. Peter C. Vollhardt |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2001 |
Journal volume | 123 |
Pages of publication | 9324 - 9337 |
a | 8.9297 ± 0.0002 Å |
b | 9.9577 ± 0.0002 Å |
c | 11.4947 ± 0.0003 Å |
α | 66.744 ± 0.001° |
β | 78.52 ± 0.002° |
γ | 79.24 ± 0.002° |
Cell volume | 913.61 ± 0.04 Å3 |
Cell temperature | 140.2 K |
Ambient diffraction temperature | 140.2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0604 |
Residual factor for significantly intense reflections | 0.0472 |
Weighted residual factors for all reflections | 0.0535 |
Weighted residual factors for significantly intense reflections | 0.0514 |
Weighted residual factors for all reflections included in the refinement | 0.0514 |
Goodness-of-fit parameter for all reflections included in the refinement | 2.014 |
Diffraction radiation wavelength | 0.7107 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4115704.html
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