Information card for entry 4115739

Structure parameters

• Formula: C14.5 H29.5 Cl N1.5 Si W0.5
• Calculated formula: C14.5 H29.5 Cl N1.5 Si W0.5
• Title of publication: Synthesis of (tBu3SiNH)2ClW\τbWCl(NHSitBu3)2 and Its Degradation via NH Bond Activation
• Authors of publication: Stephen M. Holmes; Daniel F. Schafer; Peter T. Wolczanski; Emil B. Lobkovsky
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2001
• Journal volume: 123
• Pages of publication: 10571 - 10583
• a: 11.999 ± 0.002 Å
• b: 12.801 ± 0.003 Å
• c: 23.17 ± 0.005 Å
• α: 90°
• β: 93.97 ± 0.03°
• γ: 90°
• Cell volume: 3550.4 ± 1.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0793
• Residual factor for significantly intense reflections: 0.0418
• Weighted residual factors for all reflections: 0.1203
• Weighted residual factors for significantly intense reflections: 0.0956
• Goodness-of-fit parameter for all reflections: 0.984
• Goodness-of-fit parameter for significantly intense reflections: 1.02
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No