Information card for entry 4115829

Structure parameters

• Formula: C62 H60 N10 Se11.38 Yb4
• Calculated formula: C62 H60 N10 Se11.396 Yb4
• Title of publication: Chalcogen-Rich Lanthanide Clusters: Cluster Reactivity and the Influence of Ancillary Ligands on Structure
• Authors of publication: Anna Y. Kornienko; Thomas J. Emge; John G. Brennan
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2001
• Journal volume: 123
• Pages of publication: 11933 - 11939
• a: 12.405 ± 0.006 Å
• b: 30.97 ± 0.02 Å
• c: 18.881 ± 0.01 Å
• α: 90 ± 0.06°
• β: 92.25 ± 0.04°
• γ: 90 ± 0.05°
• Cell volume: 7248 ± 7 ų
• Cell temperature: 153 ± 5 K
• Ambient diffraction temperature: 153 ± 5 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1
• Residual factor for significantly intense reflections: 0.0558
• Weighted residual factors for significantly intense reflections: 0.1409
• Weighted residual factors for all reflections included in the refinement: 0.1536
• Goodness-of-fit parameter for all reflections included in the refinement: 1.003
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No