Crystallography Open Database

Information card for entry 4115964

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Coordinates	4115964.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C34 H40 Lu N Si3
Calculated formula	C34 H40 Lu N Si3
Title of publication	C2-Symmetric ansa-Lanthanidocene Complexes. Synthesis via Silylamine Elimination and β-SiH Agostic Rigidity
Authors of publication	Jörg Eppinger; Michael Spiegler; Wolfgang Hieringer; Wolfgang A. Herrmann; Reiner Anwander
Journal of publication	Journal of the American Chemical Society
Year of publication	2000
Journal volume	122
Pages of publication	3080 - 3096
a	11.6187 ± 0.0007 Å
b	12.1293 ± 0.0008 Å
c	13.932 ± 0.0011 Å
α	78.198 ± 0.008°
β	67.611 ± 0.008°
γ	63.935 ± 0.007°
Cell volume	1629.1 ± 0.2 Å³
Cell temperature	293 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0459
Residual factor for significantly intense reflections	0.0332
Weighted residual factors for significantly intense reflections	0.0744
Weighted residual factors for all reflections included in the refinement	0.0769
Goodness-of-fit parameter for all reflections included in the refinement	0.916
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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